I was trying this once more and checking logs as it happened. This section seems to be the error:
Nov 26 19:26:42 odyssey kernel: protection error, dev sdf, sector 0 op 0x0:(READ) flags 0x80700 phys_seg 4 prio class 0
Nov 26 19:26:42 odyssey kernel: mpt3sas_cm0: log_info(0x3112043b): originator(PL), code(0x12), sub_code(0x043b)
Nov 26 19:26:42 odyssey kernel: sd 1:0:4:0: [sdf] tag#2758 UNKNOWN(0x2003) Result: hostbyte=0x05 driverbyte=DRIVER_OK cmd_age=0s
Nov 26 19:26:42 odyssey kernel: sd 1:0:4:0: [sdf] tag#2758 Sense Key : 0x5 [current]
Nov 26 19:26:42 odyssey kernel: sd 1:0:4:0: [sdf] tag#2758 ASC=0x10 ASCQ=0x3
Nov 26 19:26:42 odyssey kernel: sd 1:0:4:0: [sdf] tag#2758 CDB: opcode=0x7f, sa=0x9
Nov 26 19:26:42 odyssey kernel: sd 1:0:4:0: [sdf] tag#2758 CDB[00]: 7f 00 00 00 00 00 00 18 00 09 20 00 00 00 00 00
Nov 26 19:26:42 odyssey kernel: sd 1:0:4:0: [sdf] tag#2758 CDB[10]: 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 01
Nov 26 19:26:42 odyssey kernel: protection error, dev sdf, sector 0 op 0x0:(READ) flags 0x0 phys_seg 1 prio class 0
Nov 26 19:26:42 odyssey kernel: Buffer I/O error on dev sdf, logical block 0, async page read
Nov 26 19:26:42 odyssey emhttpd: error: ckmbr, 2291: Input/output error (5): read: /dev/sdf
Nov 26 19:26:42 odyssey emhttpd: ckmbr error: -1